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Assessment of laser induced breakdown spectroscopy accuracy for determination of hydrogen accumulation in tungsten

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dc.contributor.authorTsygvintsev, I. P.
dc.contributor.authorMarenkov, E. D.
dc.contributor.authorGasparyan, Y. M.
dc.contributor.authorStepanenko, A. A.
dc.contributor.authorМаренков, Евгений Дмитриевич
dc.contributor.authorГаспарян, Юрий Микаэлович
dc.contributor.authorСтепаненко, Александр Александрович
dc.date.accessioned2024-12-02T10:10:17Z
dc.date.available2024-12-02T10:10:17Z
dc.date.issued2021
dc.description.abstract© 2021 The Author(s)Laser-induced breakdown spectroscopy (LIBS) is an in situ method of determining hydrogen (H) content in plasma-facing materials in tokamak fusion reactors. Observing radiation from the plasma plume produced by a powerful laser pulse during the target exposition characterizes the sample composition. This is typically accomplished using the Saha-Boltzmann (SB) plot technique under local thermodynamic equilibrium (LTE) conditions. Despite many experimental studies dedicated to applying LIBS to determine H isotope retention in fusion reactor materials, the current understanding of this method's intrinsic accuracy remains inadequate. In this report, we use numerical calculations to estimate the relative error of determining H content in a sample using LIBS. As an example. we consider LIBS to study a W sample loaded with H in a vacuum. Under typical LIBS pulse parameters (109 W/cm2 and 12 ns duration), the error can be quite large, approximately 70%. We demonstrate that the error tends to decrease as the laser pulse intensity increases. Various factors contributing to the relative error are examined and their dependence on the LIBS plasma parameters is discussed. The SB plot remains a straight line even when LTE conditions are violated, making it difficult to anticipate the experimental results’ error.
dc.identifier.citationAssessment of laser induced breakdown spectroscopy accuracy for determination of hydrogen accumulation in tungsten / Tsygvintsev, I.P. [et al.] // Nuclear Materials and Energy. - 2021. - 28. - 10.1016/j.nme.2021.101029
dc.identifier.doi10.1016/j.nme.2021.101029
dc.identifier.urihttps://www.doi.org/10.1016/j.nme.2021.101029
dc.identifier.urihttps://www.scopus.com/record/display.uri?eid=2-s2.0-85107090855&origin=resultslist
dc.identifier.urihttp://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=Alerting&SrcApp=Alerting&DestApp=WOS_CPL&DestLinkType=FullRecord&UT=WOS:000691526800002
dc.identifier.urihttps://openrepository.mephi.ru/handle/123456789/25526
dc.relation.ispartofNuclear Materials and Energy
dc.titleAssessment of laser induced breakdown spectroscopy accuracy for determination of hydrogen accumulation in tungsten
dc.typeArticle
dspace.entity.typePublication
oaire.citation.volume28
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