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Бородин, Владимир Алексеевич

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Институт ядерной физики и технологий
Цель ИЯФиТ и стратегия развития - создание и развитие научно-образовательного центра мирового уровня в области ядерной физики и технологий, радиационного материаловедения, физики элементарных частиц, астрофизики и космофизики.
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Руководитель группы "Моделирование физических процессов"
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Бородин
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Владимир Алексеевич
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2019 - 201912020 - 20221
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Автор: Jublot-Leclerc, S. ×

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    Synthesis of Nano-Oxide Precipitates by Implantation of Ti, Y and O Ions in Fe-10%Cr: Towards an Understanding of Precipitation in Oxide Dispersion-Strengthened (ODS) Steels
    (2022) Jublot-Leclerc, S.; Owusu-Mensah, M.; Borodin, V. A.; Ribis, J.; Largeau, L.; Schoell, R.; Kaoumi, D.; Descoins, M.; Mangelinck, D.; Gentils, A.; Бородин, Владимир Алексеевич
    The properties of oxide dispersion-strengthened steels are highly dependent on the nature and size distribution of their constituting nano-oxide precipitates. A fine control of the processes of synthesis would enable the optimization of pertinent properties for use in various energy systems. This control, however, requires knowledge of the precise mechanisms of nucleation and growth of the nanoprecipitates, which are still a matter of debate. In the present study, nano-oxide precipitates were produced via the implantation of Y, Ti, and O ions in two different sequential orders in an Fe-10%Cr matrix that was subsequently thermally annealed. The results show that the oxides that precipitate are not necessarily favoured thermodynamically, but rather result from complex kinetics aspects related to the interaction between the implanted elements and induced defects. When Y is implanted first, the formation of nanoprecipitates with characteristics similar to those in conventionally produced ODS steels, especially with a core/shell structure, is evidenced. In contrast, when implantation starts with Ti, the precipitation of yttria during subsequent high-temperature annealing is totally suppressed, and corundum Cr2O3 precipitates instead. Moreover, the systematic involvement of {110} matrix planes in orientation relationships with the precipitates, independently of the precipitate nature, suggests matrix restriction effects on the early stages of precipitation. © 2022 by the authors.
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    In situ TEM thermal annealing of high purity Fe10wt%Cr alloy thin foils implanted with Ti and O ions
    (2019) Owusu-Mensah, M.; Jublot-Leclerc, S.; Gentils, A.; Baumier, C.; Borodin, V. A.; Бородин, Владимир Алексеевич
    © 2019 Elsevier B.V.ODS steels are ferritic-martensitic steels reinforced with (Y,Ti) oxide dispersions to enhance the creep and radiation resistance at elevated temperatures. Their conventional fabrication is achieved by ball milling followed by high-temperature consolidation. An alternative approach of ion beam synthesis has been suggested recently to study the early precipitation stages of oxide nanoparticles. To clarify the details of Ti-based oxide nanoparticle precipitation, Ti+ and O+ ions were implanted into high-purity Fe-10 wt%Cr thin foils at room temperature and subjected to thermal annealing. Nano-size oxide particles and larger surface oxide islands with pronounced Cr enrichment were observed after in situ Transmission Electron Microscopy (TEM) annealing at 600 °C and were identified as a mixed iron-chromium spinel. The features observed after ex situ annealing at 800 °C were also identified as iron-chromium oxide, but with a certain titanium enrichment. The observations thus suggest that titanium plays no major role in the early stages of oxide precipitation.